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Rapid synthesis of chitosan-capped gold nanoparticles for analytical application and facile recovery of gold from laboratory waste
Chitosan-capped gold nanoparticles (CS-AuNPs) were synthesized via a rapid method by exposing 0.75 mL of 10 mM HAuCl4 and 5 mL of 0.1% w/v chitosan solution to microwave irradiation at 125 °C for 40 s. The resulting red ...
Smartphone-based technique for the determination of a titration equivalence point from an RGB linear-segment curve with an example application to miniaturized titration of sodium chloride injections
A smartphone-based technique for determining the titration equivalence point from a linear-segment curve was developed for the first time. In this method, a titrant in an increasing microliter-volume was added to a set of ...
Investigating matrix interference in the pharmacopeial limit test for aluminum in citric acid: a re-examination, for revision of the method
In many pharmacopoeias, the limit test used for determining the level of aluminum in citric acid labeled for use in the manufacture of dialysate, is based on solvent extraction using 8-hydroxyquinoline and measurement of ...
Rapid and efficient microwave-assisted extraction of Caesalpinia sappan Linn. heartwood and subsequent synthesis of gold nanoparticles
Since microwave (MW)-assisted synthesis of gold nanoparticles (AuNPs) using Caesalpinia sappan (CS) extract as both a reducing and stabilizing agent is currently unavailable, a MW-based synthesis protocol was investigated ...
Ion pair extraction coupled with digital image colorimetry as a rapid and green platform for pharmaceutical analysis: An example of chlorpromazine hydrochloride tablet assay
Ion pair extraction coupled with digital image colorimetry has been developed as a promising platform for pharmaceutical analysis. The applicability of the approach was demonstrated through the assay of chlorpromazine ...
Smartphone-based Ellman’s colourimetric methods for the analysis of d-penicillamine formulation and thiolated polymer
A new, smartphone-based colourimetric method for the assay of d-penicillamine formulations relying on the Ellman’s reaction was developed by performing the colourimetric reaction in a microplate. Subsequently, the plate ...
Promoting student-run online class review activities as effective cooperative learning
Objectives: The aim of this work was to enable students to set up and organize for themselves online review activities after class. Materials and Methods: Students worked as groups to create short notes and quizzes that ...
Facile and green fabrication of biocatalytic chitosan beads by one-step genipin-mediated β-glucosidase immobilization for production of bioactive genistein
While glutaraldehyde is a commonly used cross-linker for enzyme immobilization, it is unsafe and requires the multi-step cross-linking procedure. Here, we report a facile, fast and cost-effective fabrication of immobilized ...
Influence of nanofiber alignment on the release of a water-soluble drug from cellulose acetate nanofibers
Cellulose acetate nanofibers with different degrees of alignment (randomly aligned (RA), partially aligned (PA), and highly aligned (HA)) were produced using an electrospinning technique. The different degrees of alignment ...